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污染物残留分析科研团队-王志发表时间:2020-07-04    作者:

污染物残留分析科研团队

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课题组长

 

 



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课题组成员


                                                            

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污染物残留分析科研团队主要从事样品前处理新技术、农兽药残留分析、环境有机污染物残留分析与控制、新型纳米材料的制备及应用等方面的研究工作。多年来,课题组在固相微萃取、聚焦微波助萃取、液相微萃取、液膜萃取、磁性固相萃取等样品前处理新技术在药物残留和污染物残留分析中的应用、石墨烯和金属-有机骨架等功能材料在色谱分析中的应用等领域开展了卓有成效的研究工作,取得了丰硕成果。近年主持完成或正在进行国家自然科学基金、河北省自然科学基金、河北省科技厅科技支撑计划、国家人事部、教育部等的科研项目20余项,获河北省自然科学二等奖二项(2009年,2013年),河北省自然科学三等奖二项(2008年,2018年)。在Analytical Chemistry、Journal of Agriculture and Food Chemistry、 Electrophoresis、Journal of chromatography A、 Analytical Chimica Acta、化学学报、分析化学等国内外重要学术刊物上发表学术研究论文260余篇,其中JCR一区、二区论文100余篇,论文被SCI他人引用总数7000余次。已培养毕业博士生5名、硕士生52名,其中2名博士生的论文获河北省优秀博士学位论文,9名硕士生的论文获河北省优秀硕士学位论文。

欢迎有志于污染物残留分析研究的同学报考本课题组研究生!

联系方式:河北农业大学理学院, 邮编071001, 电话0312-7521512

科研项目:

1. 国家自然科学基金面上项目,用于食品样品中农药残留有效萃取的新型MOF衍生孔状碳材料的制备及吸附机理研究No. 31571925,2016.1-2019.12,主持人:王志。

2. 国家自然科学基金面上项目,用于果蔬样品中农药残留分析的石墨烯复合材料涂层固相微萃取纤维的制备及其分离机理研究No. 31171698,2012-01至2015-12,主持人:王志

3. 国家自然科学基金面上项目,新型石墨烯框架材料的制备及其在一些食品中内分泌干扰物分析中的应用基础研究, 31671930,2017.1.1-2020.12,主持人:王春。

4. 国家自然科学基金面上项目,基于三维石墨烯的新型固相萃取技术体系的构建及其在食品中有害物残留分析中的应用研究No. 31471643,2015.1-2018.12,主持人:吴秋华。

5. 河北省高等学校创新团队领军人才培育计划(LJRC009)资助,痕量有机污染物检测技术体系的构建及其应用研究,2014年1月至2016年12月,主持人:王志。

6. 河北省自然科学基金, g-C3N4功能化石墨烯复合材料的制备及其在食品农药残留分析中的应用基础研究(C2018204076 ), 2018.01-2020.12,主持人:臧晓欢

7. 河北省自然科学基金, 磁性孔状碳纳米材料的制备及其在京津冀地区酞酸酯残留污染状况分析中的应用研究B2017204025, 2017.01-2019.12,主持人:吴秋华

8. 河北省自然科学基金, 磁性功能化石墨烯材料的制备及其在果蔬农药残留分析中的应用(B2012204028),2012-01至2014-12,主持人:吴秋华

9. 河北省自然科学基金,核壳型磁响应MOF复合材料的制备及其在内分泌干扰素分析中的应用基础研究B2016204136,2016.01-2018.12,主持人:王春

10. 河北省自然科学基金,青年基金项目,生物质碳材料的制备及其在农药残留分析中的应用基础研究C2017204019,2017.01-2019.12,主持人:张帅华

11. 河北省自然科学基金,青年基金,金属有机框架纳米多孔碳材料在食品中有机污染物分析中的应用B2016204146, 2016-1.-2018.12,主持人:杨秀敏

12. 河北省国际科技合作计划项目,果蔬样品中常用农药残留的新型分析技术联合研究(项目编号12396908D),2012.01-2014.12,主持人:王志

13. 河北省人力资源和社会保障厅,河北省引进留学人员择优资助项目,磁性多孔碳纳米材料的制备及其在环境、食品样品中酞酸酯残留分析中的应用研究CL201713,2017.7-2020.7,主持人:吴秋华

14. 河北省人力资源和社会保障厅,河北省人才培养工程资助经费,磁响应石墨烯纳米材料的制备及其在食品中有害物残留分析中的应用,2013年6月 至2015年12月,主持人:吴秋华

15. 河北省教育厅高等学校科学研究重点项目,用于富集环境样品中农药残留的磁性共价有机框架材料吸附剂的制备及应用研究ZD2020196,2020.1-2022.12,主持人:王志

16. 河北省教育厅高等学校科学研究重点项目,新型MOF碳材料的制备及其在京津冀地区内分泌干扰素污染状况分析中的应用研究(ZD2016085),2016-1.-2018.12,主持人:王春

17. 河北省教育厅高等学校科学研究重点项目,介孔碳增强中空纤维液相微萃取技术在抗生素残留分析中的应用ZD20131033,2013.1-2015.12,主持人:吴秋华

18. 河北省高等学校青年拔尖人才计划项目,共价有机骨架材料的制备及其吸附食品中农药残留的机理研究BJ2018024,2018年5月-2020年12月,主持人:张帅华

19. 河北省高等学校科学技术研究项目,青年基金项目,MOFs@G复合材料作为固相萃取吸附剂对有机氯环境激素的新分析方法研究QN2017085,2017.01-2019.12,主持人:臧晓欢

20. 河北省高等学校科学技术研究项目,青年基金项目,基于共价芳香聚合物的固相萃取技术体系的设计构建及其在农药残留测定中的应用研究QN2019034,2019.1-2021.12,主持人:郝琳。

21. 河北省高等学校科学技术研究,青年基金项目,用于大气可吸入颗粒中有机污染物分析的固相微萃取钛纤维的制备QN2014133,2014.3-2016.3,主持人:张帅华

 

发表的主要论文:

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发表论文他引次数

中科院一区、ESI1%高被引论文

1. Chun Wang, Cheng Feng, Yongjun Gao, Xiaoxing Ma, Qiuhua Wu, Zhi Wang*, Preparation of a graphene-based magnetic nanocomposite for the removal of an organic dye from aqueous solution, Chemical Engineering Journal, 2011, 173, 92-97. 一区,高被引论文

2. Qiuhua Wu, Guangying Zhao, Cheng Feng, Chun Wang, Zhi Wang*, Preparation of graphene-based magnetic nanocomposite for the extraction of carbamate pesticides from environmental water samples, J. Chromatogr. A, 2011, 1218, 7936– 7942. 高被引论文

3. Lu Wang, Xiaohuan Zang, Qingyun Chang, Guijiang Zhang, Chun Wang, Zhi Wang*,  Determination of Triazole fungicides in Vegetable samples by Gas Chromatography-Mass Spectrometry using graphene-coated magnetic nanocomposites as adsorbent, Food Anal Method, 2014, 7 (2),318-325. 高被引论文

4. Qianqian Wang, Chun Wang, Qiuhua Wu*, Zhi Wang*, Preparation of a magnetic nanoporous polymer for the fast and efficient extraction of 5-nitroimidazoles in milk followed by quantitation with high performance liquid chromatography-diode array detection, Journal of Agricultural and Food Chemistry, 2019, 67, 41, 11527-11535. 一区

5. Tong Wu,† Xiaohuan Zang,† Mengting Wang, Qingyun Chang, Chun Wang, Qiuhua Wu,* Zhi Wang*, Covalent Organic Framework as Fiber Coating for Solid-Phase Microextraction of Chlorophenols Followed by Quantification with Gas Chromatography−Mass Spectrometry, J. Agric. Food Chem. 2018, 66, 11158−11165. 一区

6. Yachao Pang, Xiaohuan Zang*, Hongda Li, Jinyuan Liu, Qingyun Chang,Shuaihua Zhang, Chun Wang, Zhi Wang*, Solid-phase microextraction of organophosphorous pesticides from foodsamples with a nitrogen-doped porous carbon derived from g-C3N4 templated MOF as the fiber coating, Journal of Hazardous Materials, 384 (2020) 121430. 一区  

7. Si Cheng, Qiuhua Wu*, He Xiao, Chen Hao*, Online Monitoring of Enzymatic Reactions Using Time-Resolved Desorption Electrospray Ionization Mass Spectrometry, Analytical Chemistry, 2017, 89 (4), 2338–2344. 一区

8. Shuaihua Zhang, Qian Yang, Chun Wang, Xiliang Luo, Jeonghun Kim, Zhi Wang,* Yusuke Yamauchi*, Porous organic frameworks: Advanced materials in analytical chemistry, Adv. Sci. 2018, 1801116. 一区

9. Shuaihua Zhang, Qian Yang, Wenchang Wang, Chun Wang, Zhi Wang*. Covalent bonding of metal-organic framework-5/graphene oxide hybrid composite to stainless steel fiber for solid-phase microextraction of triazole fungicides from fruit and vegetable samples [J]. Journal of Agricultural and Food Chemistry, 2016, 64, 2792-2801. 一区

10. Lin Hao, Chun Wang, Qiuhua Wu, Zhi Li, Xiaohuan Zang, and Zhi Wang*, Metal-organic framework derived magnetic nanoporous carbon: a novel adsorbent for magnetic solid-phase extraction, Anal Chem. 2014, 86(24): 12199-205. 一区

11. Chun Wang, Qiuhua Wu, Chunxia Wu, Zhi Wang*, Application of dispersion-solidification liquid-liquid microextraction for the determination of triazole fungicides in environmental water samples by high-performance liquid chromatography, Journal of Hazardous Materials, 185 (2011) 71–76.  一区

 

二区Top期刊论文

1. Gaigai Li, Junmin Wang, Qianqian Wang, Junhong Zhou, Chun Wang*, Qiuhua Wu*, Zhi Wang, A low-cost and high-efficiency carbazole-based porous organic polymer as a novel sorbent for solid-phase extraction of triazine herbicides in vegetables, Food Chemistry, 2020, 309, 125618. 二区,TOP期刊

2. Qianqian Wang1†, Chun Wang1, Junmin Wang1†, Weihua Liu, Lin Hao1, Junhong Zhou2, Qiuhua Wu1*, Zhi Wang*, Sensitive determination of phenylurea herbicides in soybean milk and tomato samples by a novel hypercrosslinked polymer based solid-phase extraction coupled with high performance liquid chromatography, Food Chemistry, 2020, 317, 126410  二区,TOP期刊

3. Wenjin Wang, Shuaihua Zhang*, Zhi Li, Jinqiu Li, Xiumin Yang, Chun Wang, Zhi Wang*, Construction of covalent triazine-based frameworks and application to solid phase microextraction of polycyclic aromatic hydrocarbons from honey samples, Food Chemistry, 2020, 322, 126770. 二区,TOP期刊

4. Qianqian Wang, Lingfang Yao, Lei Hao, Yun Li, Chun Wang, Qiuhua Wu*, Zhi Wang*, Ferrocene-based nanoporous organic polymer as solid-phase extraction sorbent for the extraction of chlorophenols from tap water, tea drink and peach juice samples, Food Chemistry 297 (2019) 124962 二区,TOP期刊

5. Shuaihua Zhang, Qian Yang, Zhi Li, Wenjin Wang, Xiaohuan Zang, Chun Wang, Zhi Wang*, Solid phase microextraction of phthalic acid esters from vegetable oils using iron (III)-based metal-organic framework/graphene oxide coating, Food Chemistry, 2018, 263, 258–264.

6. Xiaoxing Ma, Juntao Wang, Qiuhua Wu, Chun Wang, Zhi Wang*, Extraction of carbamate pesticides in fruit samples by graphene reinforced hollow fibre liquid microextraction followed by high performance liquid chromatographic detection, Food Chemistry, 2014, 157(15), 119-124. 二区,TOP期刊

7. Shuaihua Zhang, Xiumin Yang, Xiaofang Yin, Chun Wang, Zhi Wang*, Dispersive liquid–liquid microextraction combined with sweeping micellar electrokinetic chromatography for the determination of some neonicotinoid insecticides in cucumber samples, Food Chemistry, 2012, 133 (2), 544-550. 二区,TOP期刊

 

中科院二区论文

1. Tian Gao, Juntao Wang, Qiuhua Wu, Chun Wang, Zhi Wang, A Graphene Oxide–Based Composite for Solid-Phase Extraction of Carbamate Pesticides from Vegetables, Food Analytical Methods, 2020, 13(3), 690-698. 二区

2. Qianqian Wang, Gaigai Li, Chun Wang*, Qiuhua Wu*, Zhi Wang, Layered porous organic frameworks as a novel adsorbent for the solid phase extraction of chlorophenols prior to their determination by HPLC-DAD, Microchimica Acta, 2020, 187, 211. 二区

3. Yuhong Song, Di Zhang, Lin Hao, Chun Wang, Qiuhua Wu*, Zhi Wang*, Green synthesis of o-hydroxyazobenzene porous organic polymer for efficient adsorption of aromatic compounds, Journal of Chromatography A, 2019, 1583, 39-47.  二区

4. Liying Guo, Lin Hao, Tian Gao, Chun Wang*, Qiuhua Wu*, Zhi Wang, p-Phenylenediamine-modified graphene oxide as a sorbent for solid-phase extraction of phenylurea herbicides, nitroimidazoles, chlorophenols, phenylurea insecticides and phthalates, Microchimica Acta, 2019, 186, 464.  二区

5. Xiaolan Wang; Xufeng Meng; Qiuhua Wu, Chun Wang*, Zhi Wang*, Solid phase extraction of carbamate pesticides with porous organic polymer as adsorbent followed by high performance liquid chromatography-diode array detection, Journal of Chromatography A, 2019, 1600, 9-16.   二区

6. Xiaolan Wang; Tao Feng; Juntao Wang; Lin Hao; Chun Wang, Qiuhua Wu*, Zhi Wang*, Preparation of magnetic porous covalent triazine-based organic polymer for the extraction of carbamates prior to high performance liquid chromatography-mass spectrometric detection, Journal of Chromatography A, 1602 (2019) 178–187. 二区

7. Wenjin Wang, Zhi Li, Shuaihua Zhang∗, Xiumin Yang, Xiaohuan Zang, Chun Wang, Zhi Wang*, Triazine-based porous organic framework as adsorbent forsolid-phase microextraction of some organochlorine pesticides, Journal of Chromatography A, 2019, 1602, 83–90. 二区

8. Yuhong Song, Ruiyang Ma, Caina Jiao, Lin Hao, Chun Wang, Qiuhua Wu* and Zhi Wang*, Magnetic mesoporous polymelamine-formaldehyde resin as an adsorbent for endocrine disrupting chemicals, Microchim Acta, (2018) 185: 19. 二区

 9. Xinyu Liang, Juntao Wang, Qiuhua Wu, Chun Wang∗, Zhi Wang*, Use of a hypercrosslinked triphenylamine polymer as an efficient adsorbent for the enrichment of phenylurea herbicides, Journal of Chromatography A, 1538 (2018) 1–7. 二区

10. Wenchang Wang, Zhi Li, Wenjin Wang, Lihong Zhang, Shuaihua Zhang*, Chun Wang, Zhi Wang*, Microextraction of polycyclic aromatic hydrocarbons by using a stainless steel fiber coated with nanoparticles made from a porous aromatic framework, Microchim Acta, (2018) 185: 20. 二区

11. Yao Wang, Ruiyang Ma, Ruobai Xiao, Qiuhua Wu, Chun Wang*, Zhi Wang*, A hyper-cross linked polymer as an adsorbent for the extraction of chlorophenols, Microchimica Acta, 2018, 185: 108. 二区  

12. Wenchang Wang; Wenjin Wang; Shuaihua Zhang*, Zhi Li, Chun Wang, Zhi Wang*, Hyper-crosslinked polymer nanoparticles as the solid-phase microextraction fiber coating for the extraction of organochlorines, Journal of Chromatography A, 2018, 1556, 47–54. 二区

13. Xiaolan Wang, Ruiyang Ma, Lin Hao, Qiuhua Wu, Chun Wang *, and Zhi Wang*, Mechanochemical synthesis of covalent organic framework for the efficient extraction of benzoylurea insecticides, J Chromatogr A, 2018, 1551, 1-9. 二区

14. Wenjin Wang, Zhi Li, Shuaihua Zhang*, Xiumin Yang, Chun Wang, Zhi Wang*, From porous aromatic frameworks to nanoporous carbons: A novel solid phase microextraction coating, Talanta , 2018, 190, 327–334. 二区

15. Qianqian Wang, Lihong Zhang, Lin Hao, Chun Wang, Qiuhua Wu*, Zhi Wang*, Phosphorous-enriched knitting aryl network polymer for the rapid and effective adsorption of aromatic compounds, Journal of Chromatography A, 2018, 1575, 18–25.  二区

16. Yuhong Song; Ruiyang Ma; Lin Hao, Xiumin Yang, Chun Wang; Qiuhua Wu*; Zhi Wang*, Application of covalent organic framework as the adsorbent for solid-phase extraction of trace levels of pesticide residues prior to high-performance liquid chromatography-ultraviolet detection, Journal of Chromatography A, 1572 (2018) 20–26  二区

17. Tian Gao, Junmin Wang, Lin Hao, Xiumin Yang, Chun Wang*, Qiuhua Wu, Zhi Wang*, A magnetic knitting aromatic polymer as a new sorbent for use in solid-phase extraction of organics. Microchimica Acta, 2018, 185:554. 二区

18. Yachao Pang, Xiaohuan Zang*, Mengting Wang, Qingyun Chang, Shuaihua Zhang, Chun Wang, Zhi Wang*, Fibrous boron nitride nanocomposite for magnetic solid phase extraction of ten pesticides prior to the quantitation by gas chromatography. Microchimica Acta, 2018, 185:561. 二区

19. Tong Wu, Juntao Wang, Weiqian Liang, Xiaohuan Zang, Chun Wang, Qiuhua Wu*, Zhi Wang*, Single layer graphitic carbon nitride-modified graphene composite as a fiber coating for solid-phase microextraction of polycyclic aromatic hydrocarbons, Microchimica Acta, 2017, 184,2171-2180.

20. Weiqian Liang; Juntao Wang; Xiaohuan Zang; Wenhuan Dong; Chun Wang; Zhi Wang, Barley husk carbon as the fiber coating for the solid-phasemicroextraction of twelve pesticides in vegetables prior to gaschromatography–mass spectrometric detection, J. Chromatogr. A, 2017, 1491, 9-15.

21.  Caina Jiao, Ruiyang Ma, Menghua Li, Lin Hao, Chun Wang, Qiuhua Wu*, Zhi Wang* Magnetic cobalt-nitrogen-doped carbon microspheres for the preconcentration of phthalate esters from beverage and milk samples, Microchimica Acta, 2017, 184, 2551–2559.

22. Juanjuan Wu, Xinyu Liang, Lin Hao, Chun Wang*, Qiuhua Wu*, Zhi Wang, Graphene oxide cross-linked with phytic acid: an efficient adsorbent for the extraction of carbamates, Microchimica Acta, 2017, 184:3773–3779.

23. Juanjuan Wu, Ruiyang Ma, Lin Hao, Chun Wang, Qiuhua Wu, Zhi Wang,∗ Triphenylamine-based hypercrosslinked organic polymer as adsorbent for the extraction of phenylurea herbicides, Journal of Chromatography A, 2017, 1520, 48-57. 

24. Menghua Li, Juntao Wang, Caina Jiao, Chun Wang, Qiuhua Wu*, Zhi Wang, Graphene oxide framework: an adsorbent for solid phase extraction of phenylurea herbicides from water and celery samples, Journal of Chromatography A, 2016, 1469, 17–24.

25. Wenchang Wang, Juntao Wang, Shuaihua Zhang, Penglei Cui, Chun Wang, Zhi Wang, A novel Schiff base network-1 nanocomposite coated fiber for solid-phase microextraction of phenols from honey samples, Talanta 2016, 161, 22–30.

26. Xingli Liu, Chun Wang, Qiuhua Wu, Zhi Wang, Magnetic porous carbon-based solid-phase extraction of carbamates prior to HPLC analysis, Microchim Acta, 2016, 183: 415–421.

27. Caina Jiao, Menghua Li, Ruiyang Ma, Chun Wang, Qiuhua Wu, Zhi Wang, Preparation of a Co-doped hierarchically porous carbon from Co/Zn-ZIF: An efficient adsorbent for the extraction of trizine herbicides from environment water and white gourd samples, Talanta, 2016, 152(5), 321-328.